HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl Chloride → 2-Benzyltoluene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl Chloride | HCID 7503 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 2-Benzyltoluene | HCID 69738 | — |
| Produkt | Methylbis(phenylmethyl)benzene | HCID 3034397 | — |
Reaktionsschritte
In the like manner as the example in the above reference, benzyl chloride and toluene were reacted in the presence of a catalyst of FeCl3 ; and benzyltoluene and dibenzyltoluene were obtained by distillation. These benzyltoluene and dibenzyltoluene in a weight ratio of 80:20 were mixed together. The contents of isomers of the benzyltoluene in the obtained mixture were o-isomer: 39.1 wt %, m-isomer: 5.4 wt % and p-isomer: 35.5 wt %, which were almost coincident with the analytical values of the above JARYLEC C-100 of o-isomer: 36.2 wt %, m-isomer: 5.9 wt % and p-isomer: 37.8 wt %.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05134761 |
| Quelldatensatz | uspto-grants-1992_08 |
| ORD ID | ord-c55e4a3247e04bc9be651106a16733a4 |
| Quellennotiz | uspto-grants-1992_08 |