HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | O-Xylene | HCID 7237 | — |
| Edukt | Hexan-3-amine | HCID 86062 | — |
| Edukt | 4-Allyl-3-methyl-2,6-dinitrochlorobenzene | HCID 20563841 | — |
| Produkt | N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline | HCID 54001796 | — |
Reaktionsschritte
One equivalent of 4-allyl-3-methyl-2,6-dinitrochlorobenzene is dissolved in three volumes of xylene containing two equivalents of 3-hexylamine. The mixture is refluxed for 5 hours and then poured into water. The organic phase is washed with 5% hydrochloric acid and then water, dried over calcium sulfate, and removed in vacuo to leave the above-named product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04297127 |
| Quelldatensatz | uspto-grants-1981_10 |
| ORD ID | ord-930fb5109d234756b6b766f79009173a |
| Quellennotiz | uspto-grants-1981_10 |