1-Octadecene → Octadecyldichlorosilane

Beteiligte Stoffe

Reaktionsschritte

Dichlorosilane in an amount of 60.6 g (0.6 mol), 176.4 g of 1-octadecene (0.7 mol) and 0.07 mol % of RhCl(PPh)3 (relative to dichlorosilane) were charged in a 500 ml pressure-proof stainless steel reactor. After sealing, reaction was carried out at 130° C. for 30 hours. The reacted liquid was distilled in vacuo to give n-octadecyldichlorosilane (n--C18H37SiHCl2).

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