Hydrochloric Acid → HCID 178479039, Verbindung

HRID 849081

Reaktionsgleichung

Reaktionsgleichung von HRID 849081
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:3]=1.[ClH:15]>[Pt]=O>[ClH:15].[CH:9]1([CH2:8][CH:4]2[NH:3][C:2](=[NH:1])[CH2:7][CH2:6][CH2:5]2)[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 939026-Benzylpyridin-2-amine

Produkt 1

HCID 178479039HCID 178479039, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 82844Platinum oxide (PtO)Katalysator

Versuchsvorschrift

The 2-amino-6-benzylpyridine was reduced as in Example 94, except platinum oxide was used as the catalyst. The product was obtained as an oil which was dissolved in 1 N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the desired title compound as white crystals. The analysis of the product was found to be consistent with the proposed structure.

Aufarbeitung

  1. customThe product was obtained as an oil which
  2. customto give a white solid
  3. customThe solid was recrystallized from EtOAc

Quellen und Nachweise

ORD-Eintrag
ord-ab961bebbe72482badb3276f57ec740a
Quelldatensatz
uspto-grants-2000_01
Patentnummer
US06011028

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