HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzaldehyde → 1-Nitro-2-phenylethane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzaldehyde | HCID 240 | — |
| Edukt | O-Phenylenediamine | HCID 7243 | — |
| Edukt | beta-nitrostyrene, (E)- | HCID 5284459 | — |
| Produkt | 1-Nitro-2-phenylethane | HCID 80208 | 95% |
Reaktionsschritte
Example 219 A) trans-b-Nitrostyrene (63.0 g, 0.42 mole) was reacted with benzaldehyde (53.4 g, 0.5 mole) and 1,2-diaminobenzene (54.4 g, 0.5 mole) according to the procedure of Chikashita et. al. (Synth. Commun. 1985, 15 (6), 527) to yield (2-nitroethyl)benzene (60.0 g, 95%) as a yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06011028 |
| Quelldatensatz | uspto-grants-2000_01 |
| ORD ID | ord-fa6a597758a845449a7c3c11fe37506c |
| Quellennotiz | uspto-grants-2000_01 |