6-Benzylpyridin-2-amine → 2-Imino-6-cyclohexylmethylpiperidine

Beteiligte Stoffe

Reaktionsschritte

The 2-amino-6-benzylpyridine product of Example 298 A was reduced in acetic acid under hydrogen atmosphere utilizing platinum oxide catalyst to afford 2-imino-6-cyclohexylmethylpiperidine as an oil. The oil was dissolved in 1N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the title product as white crystals.

Herkunft & Nachweise