Methyl chloromethoxyacetate → Methyl 1,2,3-triazol-1-ylmethoxyacetate
Reaktionsgleichung
[NH:1]1[CH:5]=[CH:4][N:3]=[N:2]1.Cl[CH2:7][O:8][CH2:9][C:10]([O:12][CH3:13])=[O:11]>>[N:1]1([CH2:7][O:8][CH2:9][C:10]([O:12][CH3:13])=[O:11])[CH:5]=[CH:4][N:3]=[N:2]1Komponenten
3
Versuchsvorschrift
The title compound was prepared from 1,2,3-triazole and methyl chloromethoxyacetate by a similar method to that of Preparation 40 as a colourless oil which was characterised by NMR. 1H-NMR (300 MHz, CDCl3): δ=3.76 (s,3H), 4.16 (s,2H), 5.84 (s,2H), 7.80 (d,2H) ppm.
Quellen und Nachweise
- ORD-Eintrag
- ord-1831e4d6f38c42d1ac486fd9e311b0b8
- Quelldatensatz
- uspto-grants-2000_01
- Patentnummer
- US06015825
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