HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfur trioxide → 2-Methyl-5-nitrobenzenesulfonic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfur trioxide | HCID 24682 | — |
| Edukt | p-Nitrotoluene-2-sulphonic acid anhydride | HCID 53855915 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2-Methyl-5-nitrobenzenesulfonic acid | HCID 8458 | — |
Reaktionsschritte
In this procedure, the reaction mixture is obtained as a black, tarry suspension towards the end of the addition of sulphur trioxide and, after hydrolysis of the p-nitrotoluene-2-sulphonic acid anhydride with water, an aqueous solution of p-nitrotoluene-2-sulphonic acid is formed from the suspension, and this is treated with active charcoal, before or after separating off water-insoluble by-products, in order to separate off dissolved, coloured compounds and dissolved, unreacted p-nitrotoluene.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04382039 |
| Quelldatensatz | uspto-grants-1983_05 |
| ORD ID | ord-917da601c499486f9e330177f0ceb84f |
| Quellennotiz | uspto-grants-1983_05 |