HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3,4-Thiadiazol-2-amine → 2-(N-benzyloxycarbonyl-DL-isoleucylamino)-1,3,4-thiadiazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3,4-Thiadiazol-2-amine | HCID 19909 | — |
| Edukt | N-benzyloxycarbonyl-L-isoleucine | HCID 102945 | — |
| Produkt | 2-(N-benzyloxycarbonyl-DL-isoleucylamino)-1,3,4-thiadiazole | HCID 13145510 | 56,6% |
Reaktionsschritte
26.5 g of N-benzyloxycarbonyl-DL-isoleucine and 10 g of 2-amino-1,3,4-thiadiazole were reacted in the same manner as in Example 3(i) to obtain 19.5 g (yield: 56%) of 2-(N-benzyloxycarbonyl-DL-isoleucylamino)-1,3,4-thiadiazole as white crystals having a melting point of 149° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04382142 |
| Quelldatensatz | uspto-grants-1983_05 |
| ORD ID | ord-867032a5d88647ba8c89db7026dadd3d |
| Quellennotiz | uspto-grants-1983_05 |