3-(Trifluoromethyl)phenylglyoxal → N-(2-(4-Carbomethoxyphenyl)-1,1-dimethylethyl)-2-hydroxy-2-(3-trifluoromethylphenyl) ethanamine

Beteiligte Stoffe

Reaktionsschritte

The title compound was prepared as in Example 1a from 3-trifluoromethylphenyl glyoxal (2.0 g) and 2-(4-carbomethoxyphenyl)-1,1-dimethyl ethanamine (2.0 g) and crystallised from hexane m.p. 88°-90°. τ(CDCl3) 8.93 (6H,s), 6.8-8.0 (4H,m+2H replaceable by D2O), 6.1 (3H,s), 5.33 (1H,m), 2.8 (2H,d,J=8 Hz), 2.2-2.6 (4H,m), 2.03 (2H,d,J=8 Hz).

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