HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanimidic acid, N-phenyl-, ethyl ester → HCID 178482101, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanimidic acid, N-phenyl-, ethyl ester | HCID 111236 | — |
| Edukt | HCID 178507418 | HCID 178507418 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | HCID 178482101 | HCID 178482101 | 56,9% |
Reaktionsschritte
Five grams of 4-(4-aminophenyl)-1-H-imidazole were added to a solution of 4.6 gm of ethyl N-phenyl-formimidate [Org. Synth., 35, 65 (1965)] in 25 ml of acetone. After stirring for four hours at room temperature, the solid that separated was filtered and dried under vacuum. The product was treated with acetone and acidified with glacial acetic acid. N-Phenyl-N'-[4-(imidazol-4-yl]-formamidine crystallized as acetate salt which was filtered to give 4.6 gm of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04386099 |
| Quelldatensatz | uspto-grants-1983_05 |
| ORD ID | ord-5cb2b46fd81545e6a611527823935340 |
| Quellennotiz | uspto-grants-1983_05 |