HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzene, 1-fluoro-2-methyl-4-nitro- → 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)-1-(2-methyl-4-nitrophenyl)pyridin-2(1H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzene, 1-fluoro-2-methyl-4-nitro- | HCID 68001 | — |
| Edukt | 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)pyridin-2(1H)-one | HCID 59410156 | — |
| Produkt | 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)-1-(2-methyl-4-nitrophenyl)pyridin-2(1H)-one | HCID 59410212 | — |
Reaktionsschritte
Analogously to Example 4A, 1.50 g (4.13 mmol) of the compound from Example 3A are reacted with 704 mg (4.54 mmol) of 2-fluoro-5-nitrotoluene. This gives 570 mg (28% of theory) of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08846934B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-0bcd3dacdb0645a89ab81d6c03ce4396 |
| Quellennotiz | uspto-grants-2014_09 |