HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzaldehyde → 1-[2,5-Bis(2,2,2-trifluoroethoxy)phenyl]-3-phenyl-2-propen-1-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzaldehyde | HCID 240 | — |
| Edukt | 1-(2,5-Bis(2,2,2-trifluoroethoxy)phenyl)ethan-1-one | HCID 2736073 | — |
| Produkt | 1-[2,5-Bis(2,2,2-trifluoroethoxy)phenyl]-3-phenyl-2-propen-1-one | HCID 85336436 | — |
Reaktionsschritte
The title compound was prepared by heating a mixture of 2,5-bis(2,2,2-trifluoroethoxy)acetophenone (200 mg, 0.633 mmol) and benzaldehyde (64 ul, 0.633 mmol) similar to Example 1 and isolated as a yellow solid (7.2 mg, 2.8%). 1H NMR (CDCl3): 7.70 (d, J=16.2 Hz, 1H), 7.62-7.59 (m, 2H), 7.45 (d, J=15.9 Hz, 1H), 7.41 (t, J=3.2 Hz, 3H), 7.29 (d, J=3.3 Hz, 1H), 7.13 (dd, J=3.3, 9.3 Hz, 1H), 6.96 (d, J=9.0 Hz, 1H), 4.45-4.34 (m, 4H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07256219B2 |
| Quelldatensatz | uspto-grants-2007_08 |
| ORD ID | ord-3bebe27445324e85b4ccd59f41b2d312 |
| Quellennotiz | uspto-grants-2007_08 |