4-(Methoxymethoxy)benzaldehyde → 2-[(4-Methoxymethoxybenzylidene)amino]-3-methylphenol

Beteiligte Stoffe

Reaktionsschritte

2-[(4-methoxymethoxybenzylidene)amino]-3-methylphenol (F6) was prepared in a similar manner for the preparation of 2-[(5-Methoxy-2-methoxymethoxybenzylidene)amino]-3-methylphenol (F4) by using 4-methoxymethoxybenzaldehyde (F3) (3.32 g, 20 mmol) instead of 5-methoxy-2-methoxymethoxybenzaldehyde (F1) in 84% (4.56 g): 1H-NMR (500 MHz, CDCl3) δ3.53 (s, 3H), 5.24 (s, 3H), 7.17 (d, 1H, J=9.0 Hz), 7.35 (d, 1H, J=9.0 Hz), 10.52 (s, 1H).

Herkunft & Nachweise