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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 857823Erstellt: 27. Oktober 2026

Acrylic Acid → t-Butyl acrylate acrylic acid 3-hydroxypropyl methacrylate

https://huagongshe.com/reaction/857823

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcrylic AcidHCID 6581—
EduktPropylene glycol methyl ether acetateHCID 7946—
Edukttert-Butyl acrylateHCID 15458—
Edukt3-Hydroxypropyl methacrylateHCID 17694—
KatalysatorAzobisisobutyronitrileHCID 6547—
Produktt-Butyl acrylate acrylic acid 3-hydroxypropyl methacrylateHCID 86601184118,6%

Reaktionsschritte

10 g of t-butylacrylate, 4 g of acrylic acid, 6 g of 3-hydroxypropyl methacrylate and 0.4 g of AIBN were added to 200 g of PGMEA, and were then polymerized at 60° C. for 8 hours. After completion of the polymerization, the mixture was precipitated in ether, filtered, and dried in vacuo to yield 17 g of t-butyl acrylate-acrylic acid-3-hydroxypropyl methacrylate copolymer, as a white solid, represented by Formula 2 below:

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07147994B2
Quelldatensatzuspto-grants-2006_12
ORD IDord-eb8c73245c1e4136871d0a3dd29432be
Quellennotizuspto-grants-2006_12