HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester → N-(3-Amino[1,1'-biphenyl]-4-yl)-carbamic Acid tert-Butyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester | HCID 57745588 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Produkt | N-(3-Amino[1,1'-biphenyl]-4-yl)-carbamic Acid tert-Butyl Ester | HCID 57717454 | 93,4% |
Reaktionsschritte
Prepared from (3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example B5) (100 mg, 0.32 mmol) by catalytic hydrogenation with Pd/C according to the general procedure G (method a). Obtained as a white solid (85 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07151098B2 |
| Quelldatensatz | uspto-grants-2006_12 |
| ORD ID | ord-44647ca46d6a4c9c993cadb7f90ce4b2 |
| Quellennotiz | uspto-grants-2006_12 |