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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 860107Erstellt: 23. Oktober 2026

Benzaldehyde → HCID 178419005, Verbindung

https://huagongshe.com/de/reaction/860107

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzaldehydeHCID 240—
EduktAcetyl chlorideHCID 6367—
Edukt2-AminopyridineHCID 10439—
EduktTert-Butyl isocyanideHCID 23577—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178419005HCID 178419005—

Reaktionsschritte

Example 1 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07153873B2
Quelldatensatzuspto-grants-2006_12
ORD IDord-e8c0457d86b043a4a3e777f1ec561d09
Quellennotizuspto-grants-2006_12