Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 5-Chloronicotinate | HCID 6994321 | — |
| Produkt | 5-Chloronicotinic acid | HCID 247986 | 65,3% |
Reaktionsschritte
To 5-chloronicotinate (10.5 g) was added 1N NaOH (84.9 mL) at ambient temperature. The mixture was heated at 60° C. for 1 hour. The reaction mixture was adjusted to pH 4–5 with HCl. The precipitate was filtered to give 5-chloronicotinic acid (6.9 g) a colorless solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07153854B2 |
|---|
| Quelldatensatz | uspto-grants-2006_12 |
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| ORD ID | ord-537602e154b04d0cbb337da3de6eb777 |
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| Quellennotiz | uspto-grants-2006_12 |
|---|
