HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formaldehyde → Resorcinol-formaldehyde resin
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formaldehyde | HCID 712 | — |
| Edukt | Resorcinol | HCID 5054 | — |
| Produkt | Resorcinol-formaldehyde resin | HCID 159980 | — |
Reaktionsschritte
In a four-necked flask equipped with a reflux condenser and a thermometer were placed 110 g (1.0 mole) of resorcin and 44.5 g (0.55 mole) of 37% formalin, and the resulting mixture was subjected to reaction at 70° C. for five hours. The reflux condenser was then replaced by a fractionator, and the pressure in the flask was reduced to 25 mmHg, after which the temperature was elevated to 150° C., at which temperature the contents of the flask were concentrated for three hours to obtain a resorcin formaldehyde resin [T].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05717053 |
| Quelldatensatz | uspto-grants-1998_02 |
| ORD ID | ord-fabe99119f714e16a297ecd700467720 |
| Quellennotiz | uspto-grants-1998_02 |