HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tert-Butylamine → 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tert-Butylamine | HCID 6385 | — |
| Edukt | 3-Cyanoandrosta-3,5-diene-17beta-carboxylic acid | HCID 15380254 | — |
| Produkt | 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide | HCID 67646951 | 81% |
Reaktionsschritte
Following a procedure similar to that described in Preparation 16a, but using 3-cyanoandrosta-3,5-diene-17β-carboxylic acid [prepared as described in Example 1(b)] and t-butylamine as starting materials, in relative proportions similar to those used in that Preparation, the title compound was obtained in a yield of 81%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05717088 |
| Quelldatensatz | uspto-grants-1998_02 |
| ORD ID | ord-0dbbd67c48fd4b9db0ae66e1af54153b |
| Quellennotiz | uspto-grants-1998_02 |