Dicyclohexylcarbodiimide → N-(2-pyridylmethyl)benzhydrylsulphinylacetamide

Beteiligte Stoffe

Reaktionsschritte

To a suspension of 15.44 g (0.06 mol) of benzhydrylsulphinylacetic acid in 90 ml of methylene chloride are added 6.48 g (0.06 mol, i.e. 6.17 ml) of 2-aminomethylpyridine and 12.36 g (0.06 mol) of dicyclohexylcarbodiimide are added to the solution thus obtained. The mixture is heated at reflux for about 3 to 4 hours, then left to cool.

Herkunft & Nachweise