2-Bromobutanoic acid → 2-(Carbamimidoylsulfanyl)butanoic acid--hydrogen bromide (1/1)

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Reaktionsgleichung

[NH2:1][C:2]([NH2:4])=[S:3].[Br:5][CH:6]([CH2:10][CH3:11])[C:7]([OH:9])=[O:8]>>[Br-:5].[C:7]([CH:6]([S:3][C:2]([NH2:4])=[NH2+:1])[CH2:10][CH3:11])([OH:9])=[O:8]

Komponenten

Edukt 2

HCID 66552-Bromobutanoic acid

HCID 2723790Thiourea

Produkt 1

HCID 867498702-(Carbamimidoylsulfanyl)butanoic acid--hydrogen bromide (1/1)Ausbeute 79 %

Versuchsvorschrift

Example 1 was repeated with thiourea and 2-bromobutyric acid, affording the title compound in a yield of 79%.

Quellen und Nachweise

ORD-Eintrag: ord-5740b399b27c43c28b875ce39ad8c4ae
Quelldatensatz: uspto-grants-1996_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05560814

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