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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 8664Erstellt: 23. Oktober 2026

Potassium Carbonate → [2-(3-Thieno[2,3-d]isoxazol-3-yl-phenoxy)-ethyl]-thiophen-2-ylmethyl-amine

https://huagongshe.com/de/reaction/8664

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
Edukt(2-Thienylmethyl)amineHCID 34005—
Edukt3-[3-(2-Bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazoleHCID 21983582—
LösungsmittelAcetonitrileHCID 6342—
Produkt[2-(3-Thieno[2,3-d]isoxazol-3-yl-phenoxy)-ethyl]-thiophen-2-ylmethyl-amineHCID 23548223—

Reaktionsschritte

The title compound is prepared from 3-[3-(2-bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazole, potassium carbonate, C-Thiophen-2-yl-methylamine and acetonitrile essentially as described above in example 18 except that the column is eluted using a graded solvent mixture of 40% ethyl acetate in heptane, to 100% ethyl acetate. Purity by LC/MS (APCI)=100%, [M+H]+=357.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07091199B1
Quelldatensatzuspto-grants-2006_08
ORD IDord-31d4c4ba7e91456ba2cba1421a535cbb
Quellennotizuspto-grants-2006_08