HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 2,4-Diamino-6-(3-sulfamylphenyl)-s-triazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Benzoguanamine | HCID 7064 | — |
| Edukt | Chlorosulfonic acid | HCID 24638 | — |
| Produkt | 2,4-Diamino-6-(3-sulfamylphenyl)-s-triazine | HCID 20317721 | — |
Reaktionsschritte
6.0 g of benzoguanamine is heated in 30 g of chlorosulfonic acid at 130° to 140° C. for 4 hours. After cooling, the mixture is added dropwise into 300 ml of 28% aqueous ammonia with stirring and after 1 hour, the insoluble matter is filtered out and recrystallized from aqueous dimethylsulfoxide. Melting point: over 290° C.; yield: 2.0 g.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04103009 |
| Quelldatensatz | uspto-grants-1978_07 |
| ORD ID | ord-4b370c371aa94fcc940940bdf1d34c7c |
| Quellennotiz | uspto-grants-1978_07 |