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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 8675Erstellt: 24. Oktober 2026

Potassium Carbonate → (3-Methoxy-benzyl)-[2-(3-thieno[2,3-d]isoxazol-3-yl-phenoxy)-ethyl]-amine

https://huagongshe.com/de/reaction/8675

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
Edukt3-MethoxybenzylamineHCID 21156—
Edukt3-[3-(2-Bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazoleHCID 21983582—
LösungsmittelAcetonitrileHCID 6342—
Produkt(3-Methoxy-benzyl)-[2-(3-thieno[2,3-d]isoxazol-3-yl-phenoxy)-ethyl]-amineHCID 21983606—

Reaktionsschritte

The title compound is prepared from 3-[3-(2-bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazole, potassium carbonate, 3-methoxybenzylamine and acetonitrile essentially as described above in example 35, except that the column is eluted with a graded solvent mixture of 50% ethyl acetate in heptane to 100% ethyl acetate. Purity by LC/MS (APCI)=99%, [M+H]+=381.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07091199B1
Quelldatensatzuspto-grants-2006_08
ORD IDord-f69e3581a28d42ec827522042311ea49
Quellennotizuspto-grants-2006_08