Picolinic acid → Isooctadecyl picolinate

Reaktionsgleichung

[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([OH:9])=[O:8].[CH2:10](O)[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH:25]([CH3:27])[CH3:26]>>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([O:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH:25]([CH3:26])[CH3:27])=[O:8]

Komponenten

Edukt 2

HCID 1018Picolinic acid

HCID 62825Isostearyl Alcohol EX

Produkt 1

HCID 53805937Isooctadecyl picolinate

Versuchsvorschrift

Isooctadecyl picolinate was prepared using the method of Example 7 from picolinic acid and isooctadecyl alcohol, the commercial material obtained from Farbwerke Hoechst AG and described in Example 8. The light brown, oily product of the reaction had an estimated purity of 93.5%.

Quellen und Nachweise

ORD-Eintrag: ord-1c4902e866dd4c6f886fe7c80ee95705
Quelldatensatz: uspto-grants-1988_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04775763

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