Triethylene Glycol Dimethacrylate → [(Ethane-1,2-diyl)bis(oxy)ethane-2,1-diyl] bis(2-methylprop-2-enoate)--{(propane-2,2-diyl)bis[(4,1-phenylene)oxy]-2-hydroxypropane-3,1-diyl} bis(2-methylprop-2-enoate) (1/1)

HRID 868287

Reaktionsgleichung

Reaktionsgleichung von HRID 868287
[CH3:1][C:2]([C:4]([O:6][CH2:7][CH:8]([OH:37])[CH2:9][O:10][C:11]1[CH:16]=[CH:15][C:14]([C:17]([C:20]2[CH:25]=[CH:24][C:23]([O:26][CH2:27][CH:28]([OH:36])[CH2:29][O:30][C:31]([C:33]([CH3:35])=[CH2:34])=[O:32])=[CH:22][CH:21]=2)([CH3:19])[CH3:18])=[CH:13][CH:12]=1)=[O:5])=[CH2:3].[CH3:38][C:39]([C:41]([O:43][CH2:44][CH2:45][O:46][CH2:47][CH2:48][O:49][CH2:50][CH2:51][O:52][C:53]([C:55]([CH3:57])=[CH2:56])=[O:54])=[O:42])=[CH2:40]>>[CH3:3][C:2]([C:4]([O:6][CH2:7][CH:8]([OH:37])[CH2:9][O:10][C:11]1[CH:16]=[CH:15][C:14]([C:17]([C:20]2[CH:25]=[CH:24][C:23]([O:26][CH2:27][CH:28]([OH:36])[CH2:29][O:30][C:31]([C:33]([CH3:35])=[CH2:34])=[O:32])=[CH:22][CH:21]=2)([CH3:18])[CH3:19])=[CH:13][CH:12]=1)=[O:5])=[CH2:1].[CH3:40][C:39]([C:41]([O:43][CH2:44][CH2:45][O:46][CH2:47][CH2:48][O:49][CH2:50][CH2:51][O:52][C:53]([C:55]([CH3:57])=[CH2:56])=[O:54])=[O:42])=[CH2:38]

Komponenten

3

Edukt 2

HCID 7979Triethylene Glycol Dimethacrylate2×HCID 15284Bisphenol A glycidyl methacrylate2×

Produkt 1

HCID 122022[(Ethane-1,2-diyl)bis(oxy)ethane-2,1-diyl] bis(2-methylprop-2-enoate)--{(propane-2,2-diyl)bis[(4,1-phenylene)oxy]-2-hydroxypropane-3,1-diyl} bis(2-methylprop-2-enoate) (1/1)

Versuchsvorschrift

A resin/BPO stock catalyst mixture was prepared by dissolving 0.1 part of BPO in 3 parts of TEGMA and using that solution to dilute seven parts of bis-GMA to prepare a 73:0.1 mixture (all parts by weight) of bis-GMA:TEGMA:BPO. A bis-GMA/TEGMA/DHET (7:3:0.05) accelerator solution was prepared in the same way. Both solutions were kept under refrigeration until needed for further use.

Aufarbeitung

  1. customA resin/BPO stock catalyst mixture was prepared

Quellen und Nachweise

ORD-Eintrag
ord-321e733d2bc44cadb8e8f0d80d6e3825
Quelldatensatz
uspto-grants-1988_10
Patentnummer
US04778834

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