Tocotrienol → Delta-Tocotrienol

HRID 868798

Reaktionsgleichung

Reaktionsgleichung von HRID 868798
[CH3:1][C:2]([CH3:28])=[CH:3][CH2:4][CH2:5]/[C:6](/[CH3:27])=[CH:7]/[CH2:8][CH2:9]/[C:10](/[CH3:26])=[CH:11]/[CH2:12][CH2:13][C:14]1([CH3:25])[O:19][C:18]2[CH:20]=[CH:21][C:22]([OH:24])=[CH:23][C:17]=2[CH2:16][CH2:15]1.[CH3:29]CCCCC.C(OC(=O)C)C>>[CH3:29][C:20]1[C:18]2[O:19][C@@:14]([CH2:13][CH2:12]/[CH:11]=[C:10](/[CH2:9][CH2:8]/[CH:7]=[C:6](/[CH2:5][CH2:4][CH:3]=[C:2]([CH3:28])[CH3:1])\[CH3:27])\[CH3:26])([CH3:25])[CH2:15][CH2:16][C:17]=2[CH:23]=[C:22]([OH:24])[CH:21]=1

Komponenten

3

Edukt 2

HCID 9929901Tocotrienol2×HCID 21226206Ethyl acetate hexane

Produkt 1

HCID 5282350Delta-Tocotrienol

Versuchsvorschrift

Tocotrienol isomers were derived from tocotrienol rich fraction of palm oil received from First Tech International Ltd., Hong Kong and was fractionated using silica gel column chromatography with n-hexane/ethylacetate (gradient elution) as a mobile phase to yield pure δ-tocotrienol.

Quellen und Nachweise

ORD-Eintrag
ord-1207f4bd475c4ba1a9be7f654d5b7ce2
Quelldatensatz
uspto-grants-2015_03
Patentnummer
US08969303B2

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