HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-cyclopropyl-1H-1,3-benzodiazole → HCID 86721335, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-cyclopropyl-1H-1,3-benzodiazole | HCID 1084419 | — |
| Edukt | (E)-2-[8-(bromomethyl)-3-fluorodibenzo[b,e]oxepin-11(6H)-ylidene]propanenitrile | HCID 86721333 | — |
| Produkt | HCID 86721335 | HCID 86721335 | 96,3% |
Reaktionsschritte
Using 2-cyclopropyl-1H-benzo[d]imidazole (Europeane Journal of Organic Chemistry, 2000, p 1229, 69 mg, 0.434 mmol) and (E)-2-[8-(bromomethyl)-3-fluorodibenzo[b,e]oxepin-11(6H)-ylidene]propanenitrile (160 mg, 0.447 mmol) obtained in Reference Example 1, and in the same manner as in Reference Example 1A, the title compound (182 mg, 95%) was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08969345B2 |
| Quelldatensatz | uspto-grants-2015_03 |
| ORD ID | ord-5adbb5e158554deb9cb74299d2350cb2 |
| Quellennotiz | uspto-grants-2015_03 |