HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Peracetic Acid → (6-Methyl-7-oxabicyclo[4.1.0]hept-3-yl)methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Peracetic Acid | HCID 6585 | — |
| Edukt | 3-Cyclohexene-1-methanol, 4-methyl- | HCID 564672 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | (6-Methyl-7-oxabicyclo[4.1.0]hept-3-yl)methanol | HCID 86623394 | 95% |
Reaktionsschritte
Epoxidation of 12.6 g (0.1 mol) of (4-methylcyclohex-3-enyl)methanol was performed with a 5 percent by weight solution of peroxyacetic acid in ethyl acetate at 65° C. The epoxidized product was purified by distillation and thereby yielded 12 g of (6-methyl-7-oxabicyclo[4.1.0]hept-3-yl)methanol with a purity of 98%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08975349B2 |
| Quelldatensatz | uspto-grants-2015_03 |
| ORD ID | ord-31a9f14e942a47a2a60663b414812bce |
| Quellennotiz | uspto-grants-2015_03 |