HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzene → Methyl 2-nitrobenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzene | HCID 241 | — |
| Edukt | 2-Nitrobenzoic acid | HCID 11087 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Produkt | Methyl 2-nitrobenzoate | HCID 69072 | — |
Reaktionsschritte
A solution of 6-nitro-benzoic acid in benzene was treated with thionyl chloride (2.5 eq) and stirred at reflux for 8 h. After evaporation, the residue was dissolved in chloroform and then treated with methanol. After stirring at reflux for 3 h, the mixture was evaporated to afford compound 3.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08980901B2 |
| Quelldatensatz | uspto-grants-2015_03 |
| ORD ID | ord-3ab26dc5f94c470a80020d25845e6083 |
| Quellennotiz | uspto-grants-2015_03 |