Benzothiazole-6-carboxylic acid → 1-(1,3-Benzothiazol-6-yl)ethan-1-amine

HRID 876805

Reaktionsgleichung

Reaktionsgleichung von HRID 876805
[S:1]1[C:5]2[CH:6]=[C:7]([CH2:10][NH2:11])[CH:8]=[CH:9][C:4]=2[N:3]=[CH:2]1.S1C2C=C(C(O)=O)C=CC=2N=[CH:13]1.Cl.S1C2C=CN=CC=2C=C1CN>>[S:1]1[C:5]2[CH:6]=[C:7]([CH:10]([NH2:11])[CH3:13])[CH:8]=[CH:9][C:4]=2[N:3]=[CH:2]1

Komponenten

4

Edukt 3

HCID 601670Benzothiazole-6-carboxylic acidHCID 450770136-(Aminomethyl)benzothiazoleHCID 67306703Thieno[3,2-c]pyridin-2-ylmethanamine hydrochloride

Produkt 1

HCID 673051931-(1,3-Benzothiazol-6-yl)ethan-1-amine

Versuchsvorschrift

Intermediate T′ was prepared from benzo[d]thiazole-6-carboxylic acid (T-1) following similar procedures for synthesizing intermediate D′-5 from D′-1, as described above, and intermediate D from D-4 as described above. MS (m/z): 179(M+1)+.

Aufarbeitung

  1. customfor synthesizing intermediate

Quellen und Nachweise

ORD-Eintrag
ord-350c6a6ee6894cb9b23be891505c2a1f
Quelldatensatz
uspto-grants-2015_03
Patentnummer
US08987269B2

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