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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 876844Erstellt: 24. Oktober 2026

Dimethylformamide → HCID 67306428, Verbindung

https://huagongshe.com/de/reaction/876844

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDimethylformamideHCID 6228—
EduktCesium carbonateHCID 10796—
Edukt4,5,6,7-Tetrahydrothieno(3,2-c)pyridinium chlorideHCID 10176342—
EduktHCID 58514601HCID 58514601—
ProduktHCID 67306428HCID 67306428—

Reaktionsschritte

The mixture 6-((5-chloro-3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)methyl)quinoline (60 mg, 0.2 mmol) (prepared according to Compound 60), Cs2CO3 (195 mg, 0.6 mmol) and 4,5,6,7-tetrahydrothieno[3,2-c]pyridine hydrochloride (52 mg, 0.3 mmol) in DMF (1.5 mL) was stirred at 120° C. overnight, then concentrated. The residue was purified by chromatography to afford the title compound MS (m/z): 399 (M+1)+.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08987269B2
Quelldatensatzuspto-grants-2015_03
ORD IDord-c691621327fa4afd895c94af5d641f9c
Quellennotizuspto-grants-2015_03