(2,4-Dimethylphenyl)boronic acid → N-[4-(2,4-Dimethyl-phenyl)-pyridin-3-yl]-N-methyl-3,5-bis-trifluoromethyl-benzamide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	(2,4-Dimethylphenyl)boronic acid	HCID 4198739	—
Edukt	N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide	HCID 86670692	—
Produkt	N-[4-(2,4-Dimethyl-phenyl)-pyridin-3-yl]-N-methyl-3,5-bis-trifluoromethyl-benzamide	HCID 86670693	—

Reaktionsschritte

The title compound was prepared in analogy to example 25, from N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide (example 25, intermediate a) and 2,4-dimethylbenzeneboronic acid (CAS RN 55499-44-0). Colorless solid (52%). MS (ESI): m/z=453.4 [M+H]+.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08987307B2
Quelldatensatz	uspto-grants-2015_03
ORD ID	ord-71812d9cb4ce4263b8c1f50200517682
Quellennotiz	uspto-grants-2015_03