4-Methoxy-3-(trifluoromethyl)benzoic acid → HCID 70663270, Verbindung

HRID 878085

Reaktionsgleichung

Reaktionsgleichung von HRID 878085
[CH3:1][NH:2][C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH3:15].[CH3:16][O:17][C:18]1[CH:26]=[CH:25][C:21]([C:22]([OH:24])=O)=[CH:20][C:19]=1[C:27]([F:30])([F:29])[F:28]>>[CH3:16][O:17][C:18]1[CH:26]=[CH:25][C:21]([C:22]([N:2]([CH3:1])[C:3]2[CH:4]=[N:5][CH:6]=[CH:7][C:8]=2[C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[CH3:15])=[O:24])=[CH:20][C:19]=1[C:27]([F:30])([F:29])[F:28]

Komponenten

3

Edukt 2

HCID 27752954-Methoxy-3-(trifluoromethyl)benzoic acidHCID 18403336N-methyl-4-o-tolylpyridin-3-amine

Produkt 1

HCID 70663270HCID 70663270, Verbindung

Versuchsvorschrift

The title compound was prepared in analogy to example 90, from N-methyl-4-o-tolylpyridin-3-amine (example 1, intermediate a) and 4-methoxy-3-(trifluoromethyl)benzoic acid (CAS RN 213598-09-5) after a reaction time of 88 hours. Brown solid (4%). MS (ESI): m/z=401.15 [M+H]+.

Quellen und Nachweise

ORD-Eintrag
ord-b8e8a74ea59244f0bea3083d3a42b187
Quelldatensatz
uspto-grants-2015_03
Patentnummer
US08987307B2

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