HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → Benzyl 4-chlorobenzoyloxycarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Edukt | Benzyl hydroxycarbamate | HCID 18907 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | Benzyl 4-chlorobenzoyloxycarbamate | HCID 51033117 | — |
Reaktionsschritte
4-Chlorobenzoyl chloride (13.1 mL, 102 mmol) is added slowly to a solution of benzyl hydroxycarbamate (19.0 g, 114 mmol) and triethylamine (14.4 mL, 104 mmol) in diethyl ether (500 mL) at 0° C. then stirred at room temperature for 1 h. The reaction is
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08987504B2 |
| Quelldatensatz | uspto-grants-2015_03 |
| ORD ID | ord-61ae2cfa3efb4b06b28f8c9207977e98 |
| Quellennotiz | uspto-grants-2015_03 |