HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,7-Diphenyl-4-heptanol → HCID 178418375, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,7-Diphenyl-4-heptanol | HCID 10539870 | — |
| Edukt | HCID 178418459 | HCID 178418459 | — |
| Edukt | HCID 178418471 | HCID 178418471 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | HCID 178418375 | HCID 178418375 | — |
Reaktionsschritte
The alcohol 137 was prepared from the crude aldehyde 136. and 1.5 mL (0.75 mmol) of 120 in 2.0 mL of THF as described above for the synthesis of alcohol 121 in Example 1 to give 220 mg of the crude diastereomeric alcohol 137. Flash chromatography (elution with 20% ethyl acetate in hexane) afforded 146 mg of the alcohol 137 as an oil. 1H NMR consistent with structure.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05723459 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-a6be5895ebf2488a874923e3878acfbe |
| Quellennotiz | uspto-grants-1998_03 |