1,3-Benzenedisulfonamide → HCID 22244643, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23](=[O:31])OC3C=CC=CC=3)=[CH:16][CH:15]=2)[N:3]=1.[C:32]1([S:42]([NH2:45])(=[O:44])=[O:43])[CH:37]=[CH:36][CH:35]=[C:34]([S:38]([NH2:41])(=[O:40])=[O:39])[CH:33]=1>>[CH3:1][C:2]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[C:5]([CH3:13])[N:4]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][NH:22][C:23]([NH:45][S:42]([C:32]3[CH:37]=[CH:36][CH:35]=[C:34]([S:38]([NH2:41])(=[O:40])=[O:39])[CH:33]=3)(=[O:44])=[O:43])=[O:31])=[CH:16][CH:15]=2)[N:3]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 1,3-benzenedisulfonamide: 1H-NMR (CDCl3) δ 8.47 (1H, s), 8.05-7.95 (2H, m), 7.52-7.09 (10H, m), 6.27 (1H, br.s), 3.37-3.28 (2H, m), 2.75-2.64 (2H, m), 2.17 (3H, s), 2.13 (3H, s).
Quellen und Nachweise
- ORD-Eintrag
- ord-c418b7f9c3c2434c9616197ef0e5ac87
- Quelldatensatz
- uspto-grants-2006_02