3,4-Dimethoxyphenylboronic acid → HCID 22244574, Verbindung
Reaktionsgleichung
I[C:2]1[C:3]([CH3:17])=[N:4][N:5]([C:8]2[CH:13]=[CH:12][C:11]([CH2:14][CH2:15][OH:16])=[CH:10][CH:9]=2)[C:6]=1[CH3:7].[CH3:18][O:19][C:20]1[CH:21]=[C:22](B(O)O)[CH:23]=[CH:24][C:25]=1[O:26][CH3:27]>>[CH3:18][O:19][C:20]1[CH:21]=[C:22]([C:2]2[C:3]([CH3:17])=[N:4][N:5]([C:8]3[CH:13]=[CH:12][C:11]([CH2:14][CH2:15][OH:16])=[CH:10][CH:9]=3)[C:6]=2[CH3:7])[CH:23]=[CH:24][C:25]=1[O:26][CH3:27]Komponenten
3
Versuchsvorschrift
The title compound was prepared according to the procedure described in step 1 of Example 12 from 2-[4-(4-iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol (step 2 of Example 11) and 3,4-dimethoxyphenylboronic acid: MS (ESI) m/z 353 [M+H]+.
Quellen und Nachweise
- ORD-Eintrag
- ord-c2b98995d65944ecbdac4fc1400b098e
- Quelldatensatz
- uspto-grants-2006_02
- Patentnummer