HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glyoxylic Acid → HCID 11259991, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glyoxylic Acid | HCID 760 | — |
| Edukt | Borate | HCID 26574 | — |
| Edukt | (-)-Cystine | HCID 67678 | — |
| Produkt | HCID 11259991 | HCID 11259991 | — |
Reaktionsschritte
The alternative route, relying on in solution phase synthesis of an intermediate product starts with addition of a large excess (40 times) of glyoxylic acid to L-cystine in an alkaline borate buffer. The intermediate product was thereafter, after pH manipulations and conductivity adjustment of the reaction mixture, purified with ion exchange chromatography to give N,N,N′,N′-tetrakis (carboxymethyl)-L-cystine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07005071B2 |
| Quelldatensatz | uspto-grants-2006_02 |
| ORD ID | ord-ce089f0ba7b44eafb0e7bc10f2374c60 |
| Quellennotiz | uspto-grants-2006_02 |