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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 893430Erstellt: 24. Oktober 2026

Methanol → 4-(2-Methoxyethyl)phenol

https://huagongshe.com/de/reaction/893430

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethanolHCID 887—
Edukt4-Hydroxyphenylglyoxal dimethyl acetalHCID 19788847—
EduktHCID 178418361HCID 178418361—
KatalysatorPalladiumHCID 23938—
Produkt4-(2-Methoxyethyl)phenolHCID 9251659%

Reaktionsschritte

The procedure of Example 2 was repeated with a solution of 3.00 g (15.3 mmol) 4-hydroxyphenylglyoxal dimethyl acetal in 10 g methanol containing 0.16 g (4.4 mmol) hydrogen chloride and 0.15 g moist 10% Pd/C catalyst being reacted with hydrogen gas pressurized at 300 psig at 50° C. 300 rpm. A 59% yield of 4-(2'-methoxyethyl)phenol was obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05124489
Quelldatensatzuspto-grants-1992_06
ORD IDord-c8d27b60dd4f4624ba1f8e4193a867b2
Quellennotizuspto-grants-1992_06