HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanol → 4-(2-Methoxyethyl)phenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | 4-Hydroxyphenylglyoxal dimethyl acetal | HCID 19788847 | — |
| Produkt | 4-(2-Methoxyethyl)phenol | HCID 92516 | 47% |
Reaktionsschritte
The procedure of Example 2 was repeated with a solution of 2.00 g (10.2) mmol) 4-hydroxyphenylglyoxal dimethyl acetal in 10 g methanol containing 0.37 g (10.2 mmol) hydrogen chloride and a 0.20 g dry 10% Pd/C catalyst being reacted with hydrogen gas pressurized at 50 psig at 25° C. A 47% yield of 4-(2'-methoxyethyl)phenol was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05124489 |
| Quelldatensatz | uspto-grants-1992_06 |
| ORD ID | ord-d12f1b3bc7654c74aa26163577d4b7bc |
| Quellennotiz | uspto-grants-1992_06 |