HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pyridine → 1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pyridine | HCID 1049 | — |
| Edukt | Trityl chloride | HCID 6456 | — |
| Edukt | 3-(2-Hexyl-4-tetradecylphenoxy)-1,2-propanediol | HCID 14819670 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanol | HCID 15030267 | — |
Reaktionsschritte
A mixture of 11.64 g of 3-(2-hexyl-4-tetradecylphenoxy)-1,2-propanediol, 12.32 g of trityl chloride and 40 ml of pyridine was stirred for 24 hours, then diluted with chloroform, washed with aqueous sodium bicarbonate, water, dried and the solvents evaporated under reduced pressure. The residue was coevaporated with toluene giving 14.6 g of the desired compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05126291 |
| Quelldatensatz | uspto-grants-1992_06 |
| ORD ID | ord-41ad95243d594b56b1a757334baa74eb |
| Quellennotiz | uspto-grants-1992_06 |