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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 893592Erstellt: 25. Oktober 2026

Pyridine → 1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanol

https://huagongshe.com/reaction/893592

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPyridineHCID 1049—
EduktTrityl chlorideHCID 6456—
Edukt3-(2-Hexyl-4-tetradecylphenoxy)-1,2-propanediolHCID 14819670—
LösungsmittelChloroformHCID 6212—
Produkt1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanolHCID 15030267—

Reaktionsschritte

A mixture of 11.64 g of 3-(2-hexyl-4-tetradecylphenoxy)-1,2-propanediol, 12.32 g of trityl chloride and 40 ml of pyridine was stirred for 24 hours, then diluted with chloroform, washed with aqueous sodium bicarbonate, water, dried and the solvents evaporated under reduced pressure. The residue was coevaporated with toluene giving 14.6 g of the desired compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05126291
Quelldatensatzuspto-grants-1992_06
ORD IDord-41ad95243d594b56b1a757334baa74eb
Quellennotizuspto-grants-1992_06