Benzonitrile, 4-(trifluoromethyl)- → 4-Methylbenzotrifluoride

HRID 893826

Reaktionsgleichung

Reaktionsgleichung von HRID 893826
[F:1][C:2]([F:12])([F:11])[C:3]1[CH:10]=[CH:9][C:6]([C:7]#N)=[CH:5][CH:4]=1>CO>[F:1][C:2]([F:11])([F:12])[C:3]1[CH:4]=[CH:5][C:6]([CH3:7])=[CH:9][CH:10]=1

Komponenten

3

Edukt 1

HCID 67995Benzonitrile, 4-(trifluoromethyl)-

Produkt 1

HCID 802304-MethylbenzotrifluorideAusbeute 91 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel2×

Versuchsvorschrift

To 4 ml of methanol (3.06 g) was added 0.71 g of p-trifluoromethylbenzonitrile. The solution was added to the reactor at 0.34 ml/min. The product, p-trifluoromethyltoluene, was isolated in a methanol solution in a 91% yield.

Aufarbeitung

  1. additionThe solution was added to the reactor at 0.34 ml/min

Quellen und Nachweise

ORD-Eintrag
ord-84acf6a8785148ce8de82354af2abfe6
Quelldatensatz
uspto-grants-1992_06
Patentnummer
US05126497

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