Acrylonitrile → 9-(2-Cyanoethyl)-9H-fluorene-9-carboxamide

Beteiligte Stoffe

Reaktionsschritte

Five hundred g. of 9-carbamoylfluorene was slurried in 13 liters of tetrahydrofuran under nitrogen, and the mixture was stirred and heated to 50°. Fifty ml. of Triton B was added, followed by 131 g. of acrylonitrile. The mixture was stirred at 50° for 6 hours, and 65 g. of additional acrylonitrile and 25 ml. of Triton B were added. The mixture was stirred at 50° overnight.

Herkunft & Nachweise