Hydrazine → HCID 136359185, Verbindung
Reaktionsgleichung
[CH3:1][C:2]12[CH2:12][CH2:11][CH:5]([C:6](=[N:9][OH:10])[C:7]1=O)[CH:4]([CH3:13])[O:3]2.[NH2:14][NH2:15]>C(O)C>[CH3:1][C:2]12[CH2:12][CH2:11][CH:5]([C:6](=[N:9][OH:10])[C:7]1=[N:14][NH2:15])[CH:4]([CH3:13])[O:3]2Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A mixture of 1.83 g. (0.01 mole) 1,3-dimethyl-2-oxabicyclo[2,2,2]octan-5,6-dione-5-oxime and 0.35 ml. (0.011 mole) anhydrous hydrazine (98%) in 25 ml. absolute ethanol is refluxed under nitrogen at a bath temperature of 80° C. for 1 hour. Evaporation of the solvent gives 1,3-dimethyl-2-oxa-bicyclo[2,2,2]octan-5,6-dione-5-oxime-6-hydrazone.
Aufarbeitung
- additionA mixture of 1.83 g
- customEvaporation of the solvent
Quellen und Nachweise
- ORD-Eintrag
- ord-777b7eee3d114927a507276c06dc3c71
- Quelldatensatz
- uspto-grants-1981_08
- Patentnummer
- US04285944
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