1-Chloro-2-methoxy-6-(4-methoxyphenyl)naphthalene → 1-Chloro-6-(4-hydroxyphenyl)-2-naphthol
Reaktionsgleichung
[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([C:12]3[CH:17]=[CH:16][C:15]([O:18]C)=[CH:14][CH:13]=3)=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[O:20]C.Cl.[NH+]1C=CC=CC=1>>[Cl:1][C:2]1[C:11]2[C:6](=[CH:7][C:8]([C:12]3[CH:17]=[CH:16][C:15]([OH:18])=[CH:14][CH:13]=3)=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[OH:20]Komponenten
3
Versuchsvorschrift
The title compound was prepared by reacting 1-chloro-2-methoxy-6-(4-methoxyphenyl)naphthalene (0.32 g, 1.07 mmol) with pyridinium HCl (7 g) at 190° C. according to method B to yield 0.12 g (41%) of an off white solid: mp 222-224° C. (dec.);
Aufarbeitung
- customat 190° C.
- customto yield 0.12 g (41%) of an off white solid
Quellen und Nachweise
- ORD-Eintrag
- ord-e71de5fa2a594b95ab954da6a586fd94