HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Trifluoroacetic acid → (4-{2-[2-(Methoxycarbonyl)phenoxy]ethyl}phenoxy)acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Trifluoroacetic acid | HCID 6422 | — |
| Edukt | Methyl 2-{2-[4-(2-tert-butoxy-2-oxoethoxy)phenyl]ethoxy}benzoate | HCID 69259306 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | (4-{2-[2-(Methoxycarbonyl)phenoxy]ethyl}phenoxy)acetic acid | HCID 69258392 | 95% |
Reaktionsschritte
Methyl 2-{2-[4-(2-tert-butoxy-2-oxoethoxy)phenyl]ethoxy}benzoate (0.400 g, 1.0351 mmol) was dissolved in DCM and trifluoracetic acid (0.8 ml, 8.281 mmol) was added. The mixture was stirred at room temperature for 3 h. The solvent was evaporated to give 325 mg of a white powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07351858B2 |
| Quelldatensatz | uspto-grants-2008_04 |
| ORD ID | ord-03c3e0039056428a82fe06c4ce0e4358 |
| Quellennotiz | uspto-grants-2008_04 |