HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Ethoxypyridin-3-amine → (6-Ethoxy-pyridin-3-yl)-isopropyl-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Ethoxypyridin-3-amine | HCID 3040301 | — |
| Edukt | 6-chloro-N-(propan-2-yl)pyridin-3-amine | HCID 58957920 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | (6-Ethoxy-pyridin-3-yl)-isopropyl-amine | HCID 58957938 | — |
Reaktionsschritte
Following the procedure described for Preparation 2(A), 6-ethoxy-pyridin-3-ylamine (10 g, 72.4 mmol) was reacted with acetone (4.8 mL) to provide 11.18 g of (6-ethoxy-pyridin-3-yl)-isopropyl-amine. 1H NMR (CD3OD) δ 7.48 (d, 1H), 7.11 (dd, 1H), 6.61 (d, 1H), 4.14 (q, 2H), 3.48 (m, 1H), 1.32 (t, 3H), 1.14 (d, 6H); MS 181.3 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07358242B2 |
| Quelldatensatz | uspto-grants-2008_04 |
| ORD ID | ord-962deba8319d4c39a96ddbc4e6364ddd |
| Quellennotiz | uspto-grants-2008_04 |