Ethanol → N,N'-Dimethoxy-N,N'-dimethyloxamide

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Reaktionsgleichung

[CH2:1]([OH:3])C.C[N:5]([CH3:8])[CH:6]=[O:7]>>[CH3:1][O:3][N:5]([CH3:8])[C:6]([C:6]([N:5]([O:3][CH3:1])[CH3:8])=[O:7])=[O:7]

Komponenten

Edukt 2

HCID 702Ethanol

HCID 6228Dimethylformamide

Produkt 1

HCID 3287678N,N'-Dimethoxy-N,N'-dimethyloxamideAusbeute 77,5 %

Versuchsvorschrift

The reaction was carried out in the same manner as in Example 3 except for changing ethanol to dimethylformamide in Example 3. As a result, 1.16 g (Reaction yield: 77.5%) of N,N′-dimethoxy-N,N′-dimethyl oxamide was found to be formed.

Quellen und Nachweise

ORD-Eintrag: ord-a7273332ab1b49f88a34ff901c81eb6f
Quelldatensatz: uspto-grants-2008_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07358394B2

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